QCSs

The batches obtained for standards defined as Quality Controlled Standards (QCSs) do not allow carrying out all the study requirements due to the limited size. However, they have been developed following the guidelines of ISO Guides Series 30, and the analytical method for quantification and assignment of purity is liquid chromatography coupled to ESI-MS/MS.

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QCSs

Azaspiracid-4

02-AZA4

Code: 02-AZA4 Lot: 20-001 Aprox size: 0.5 µg In: 0.5 mL Material Specification CONCENTRATION: (1.31 ± 0.03) µg/mL PURITY: ≥98% FORMULATION: Liquid. In methanol. SHIPPING: SHIPPED ON ICE LONG TERM STORAGE: -20°C

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QCSs

Azaspiracid-5

02-AZA5

Code: 02-AZA5 Lot: 21-001 Aprox size 0.5 µg In: 0.5 mL CONCENTRATION: (1.26 ± 0.09) µg/mL PURITY: ≥95% FORMULATION: Liquid. In methanol. SHIPPING: SHIPPED ON ICE LONG TERM STORAGE: -20°C

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QCSs

13,19-didesmethyl spirolide C

00-13,19-didesMeC

Code: 00-13,19-didesMeC Lot:20-001 Aprox size 3.5 µg In: 0.5 mL CONCENTRATION: (7.53 ± 0.57) µg/mL PURITY: ≥95%† FORMULATION: Liquid. In methanol with TFA 0.05% v/v SHIPPING: SHIPPED ON ICE LONG TERM STORAGE: -20°C

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QCSs

13-desmethyl spirolide C

00-13desMeC

Code: 00-13desMeC Lot: 22-001 Aprox size 3.5 µg In: 0.5 mL CONCENTRATION: (7.28 ± 0.30) µg/mL PURITY: ≥99%† FORMULATION: Liquid. In methanol with TFA 0.05% v/v SHIPPING: SHIPPED ON ICE LONG TERM STORAGE: -20°C

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QCSs

20-methyl spirolide G

00-SPX20G

Code: 00-SPX20G Lot: 23-001 Aprox size 3.3 µg In: 0.5 mL Material Specification CONCENTRATION: (6.67 ± 0.16) µg/mL PURITY: ≥99% FORMAT: Amber glass vial (approx. 0.5 ml) FORMULATION: Liquid. In methanol with TFA 0.05% v/v LONG TERM STORAGE: -20°C

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QCSs

Gambierone

00-GAM

Code: 00-GAM Lot: 20-001 Aprox size: 10 µg In: 0.5 mL Material Specification CONCENTRATION: (19.9 ± 0.6) µg/mL PURITY: ≥98% FORMAT: Amber glass vial (approx. 0.5 ml) FORMULATION: Liquid. In methanol. SHIPPING: SHIPPED ON ICE LONG TERM STORAGE: -20°C

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QCSs

44-methyl-Gambierone

00-44MeGAM

Code: 00-44MeGAM Lot: 20-001 Aprox size: 10 µg In: 0.5 mL Material Specification CONCENTRATION: (19.9 ± 0.5) µg/mL PURITY: ≥97% FORMAT: Amber glass vial (approx. 0.5 ml) FORMULATION: Liquid. In methanol. SHIPPING: SHIPPED ON ICE LONG TERM STORAGE: -20°C

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